Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Methyl 4-benzyloxybenzimidate hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Tetrahydrofuran | HCID 8028 | — |
| 반응물 | 4-Benzyloxybenzonitrile | HCID 561371 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 4-benzyloxybenzimidate hydrochloride | HCID 12222189 | — |
반응 단계
A solution of 560 mg of 4-benzyloxybenzonitrile in 16 ml of THF and 0.2 ml of methanol, cooled to 0° C., was saturated with hydrogen chloride and kept at 4° C. for 16 hours. The precipitate was filtered off, washed with diethyl ether and dried to give 357 mg of methyl 4-benzyloxybenzimidate hydrochloride, m.p. 179°-180° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05057614 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-7456a4145aae444eb85ca8084af499b7 |
| 출처 메모 | uspto-grants-1991_10 |