HCID 15070022, 화합물 → 2-Methyl-4-oxa-2,8-diazabicyclo[4.3.0]nonane
반응식
[CH3:1][N:2]1[CH2:10][O:9][CH2:8][CH:7]2[CH:3]1[CH2:4][N:5](C(OCC)=O)[CH2:6]2>O>[CH3:1][N:2]1[CH2:10][O:9][CH2:8][CH:7]2[CH:3]1[CH2:4][NH:5][CH2:6]2참가 물질
3
실험 절차
9 g (42 mmol) of ethyl 2-methyl-4-oxa-2,8-diazabicyclo[4.3.0]nonane-8-carboxylate are heated under reflux with 28 g of Ba(OH)2.8H2O in 280 ml of water overnight. The BaCO3 is filtered off with suction, the filtrate is concentrated and the residue is boiled up with dioxane. The dioxane solution is concentrated and the residue is distilled.
후처리
- filtrationThe BaCO3 is filtered off with suction
- concentrationthe filtrate is concentrated
- concentrationThe dioxane solution is concentrated
- distillationthe residue is distilled
출처 및 근거
- ORD 기록
- ord-6f6007457c2e4818a86c1d4859628d37
- 출처 데이터셋
- uspto-grants-1991_10
- 특허 번호
- US05059597
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