Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tridecanoic acid → Tridecanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tridecanoic acid | HCID 12530 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | Tridecanoyl chloride | HCID 87288 | — |
반응 단계
To a benzene solution containing 5.0 g (0.023 mol) of tridecanoic acid was added 25 g of thionyl chloride, followed by refluxing for 5 hours. The excess of thionyl chloride and benzene were removed by distillation to obtain tridecanoyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05059628 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-b6fd7f8ab8d244baa08dccc98c1036ee |
| 출처 메모 | uspto-grants-1991_10 |