Vinylidene fluoride → 2-Trifluoromethyl-1,1,1,2,4,4-hexafluorobutane

반응식

[F:1][C:2]([F:13])([F:12])[CH:3]([CH2:8][CH:9]([F:11])[F:10])[C:4]([F:7])([F:6])[F:5].[F:14]C(F)=C>>[F:1][C:2]([F:12])([F:13])[C:3]([F:14])([CH2:8][CH:9]([F:10])[F:11])[C:4]([F:6])([F:5])[F:7]

참가 물질

반응물 2

HCID 6369Vinylidene fluoride

HCID 19888728Butane, 1,1,1,4,4-pentafluoro-2-(trifluoromethyl)-

생성물 1

HCID 199315252-Trifluoromethyl-1,1,1,2,4,4-hexafluorobutane

실험 절차

As another example, 2-trifluoromethyl-1,1,1,4,4-pentafluorobutane may be prepared by reacting commercially available 1,1-difluoroethylene according to the procedure of George L. Fleming et al., supra, to form a product which may then be hydrogenated to form 2-trifluoromethyl-1,1,1,2,4,4-hexafluorobutane which may then be dehydrohalogenated and then hydrogenated to form 2-trifluoromethyl-1,1,1,4,4-pentafluorobutane

후처리

customFleming et al., supra, to form a product which

출처 및 근거

ORD 기록: ord-32b8ce0597584de38ba0a96c2c749f3f
출처 데이터셋: uspto-grants-1991_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05059728

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