Barium hydroxide → Thiomandelic acid

HRID 346245

반응식

HRID 346245 반응식
[C:1]1([CH:7]2[S:11]C(=N)N[C:8]2=[O:13])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-:14].[Ba+2].[OH-]>C(O)C>[SH:11][CH:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[C:8]([OH:13])=[O:14]

참가 물질

4

반응물 2

HCID 6093286Barium hydroxideHCID 1356332132-Amino-5-phenyl-1,3-thiazol-4-one

생성물 1

HCID 10464709Thiomandelic acid수율 70%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Hydrolysis of 142 g of 5-phenyl-2-imino-4-thiazolidinone with barium hydroxide in 20% aqueous ethanol gave 55 g of α-mercaptophenylacetic acid (70% yield).

출처 및 근거

ORD 기록
ord-acdc8c1a458d4119a821fc56cfb443ee
출처 데이터셋
uspto-grants-1991_10
특허 번호
US05061720

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