Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Azobisisobutyronitrile → Methacrylic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | Methacrylate | HCID 87595 | — |
| 반응물 | Fluoro acrylate | HCID 21909953 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | Methacrylic Acid | HCID 4093 | — |
| 생성물 | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
반응 단계
This example illustrates conjoint use of the fluoro acrylate and methacrylate. 75.81 g (40.8 wt. %) of the perfluoroalkyl methacrylate (DuPont's Zonyl-TM), 72.3 g (38.9 wt. %) of the perfluoroalkyl acrylate (Hoechst-Celanese NUVA HF), 17.61 g (9.5 wt. %) of methacrylic acid, and 19.98 g (10.8 wt. %) of 2-hydroxyethyl methacrylate were polymerized in 300 ml THF, using 0.55 g AIBN as initiator, employing above-described procedure. Yield: 79.1%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05061769 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-cd1e6f295915444e88010f80a06c0170 |
| 출처 메모 | uspto-grants-1991_10 |