반응식
[CH:1](Cl)([O:6][CH:7]([F:9])[F:8])[C:2]([F:5])([F:4])[F:3].[F-:11].[K+]>>[CH:7]([O:6][CH:1]([C:2]([F:5])([F:4])[F:3])[F:11])([F:9])[F:8]참가 물질
3
반응 조건
- 온도
- 195 °C
실험 절차
12.9 g of isoflurane (FORANE® isoflurane commercially available from Anaquest Division of BOC, Inc. in Madison, Wis.) were combined with 5.5 g of potassium fluoride and 20 ml of diethylglycol and the mixture was heated with stirring for 10 hours in a glass pressure vessel at 195° C. The heated mixture was washed with ice water and the organic layer was subjected to gas chromatography, which showed the presence of the compound CHF2OCHFCF3 (29% yield).
후처리
- temperaturethe mixture was heated
- washThe heated mixture was washed with ice water
출처 및 근거
- ORD 기록
- ord-18aec9d14c6b448389c5aa7c859e12fe
- 출처 데이터셋
- uspto-grants-1988_08
- 특허 번호
- US04762856
연결된 노트
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