Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyrrolidine → BOC-L-methionyl-pyrrolidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyrrolidine | HCID 31268 | — |
| 반응물 | Boc-L-methionine | HCID 89857 | — |
| 생성물 | BOC-L-methionyl-pyrrolidine | HCID 11034003 | — |
반응 단계
2.50 g (10 mmol) BOC-methionine was coupled to 1.72 ml (20.6 mmol) pyrrolidine according to procedure B. Yield of crude product 3.38 g. The product was purified with a silica column using ethyl acetate as eluent. Yield 2.81 g (9.3 mmol, 93%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07173024B2 |
| 출처 데이터셋 | uspto-grants-2007_02 |
| ORD ID | ord-b0b858eef19d47ada090bbefcb651833 |
| 출처 메모 | uspto-grants-2007_02 |