참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium sulfite heptahydrate | HCID 160916 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | 6-Chloronaphthalene-2-sulfonyl chloride | HCID 10635129 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 23704948 | HCID 23704948 | 96.6% |
반응 단계
6-Chloronaphth-2-ylsulphonyl chloride (2.61 g) was added in one portion to a stirred mixture of sodium sulphite heptahydrate (4.71 g), sodium bicarbonate (1.64 g) and water (25 ml) which had been heated to 70° C. The resultant mixture was heated to that temperature for 3 hours and then allowed to cool slowly to ambient temperature. The crystalline precipitate was isolated giving sodium 6-chloronaphth-2-ylsulphinate (2.4 g) which was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07173025B1 |
|---|
| 출처 데이터셋 | uspto-grants-2007_02 |
|---|
| ORD ID | ord-479b1b54406f4419abd03e4c28b8b5b5 |
|---|
| 출처 메모 | uspto-grants-2007_02 |
|---|
