Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → HCID 21850022, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 2,4-Diaminopyrimidine-5-carbaldehyde | HCID 309176 | — |
| 반응물 | 2,4,6-Trimethylphenylacetonitrile | HCID 520698 | — |
| 용매 | Methane | HCID 297 | — |
| 생성물 | HCID 21850022 | HCID 21850022 | — |
반응 단계
The title compound was prepared according to Example 1, starting from 0.915 g of 2,4,6-trimethyl-benzyl cyanide and 0.76 g of 2,4-diamino-5-pyrimidine-carboxaldehyde; mp 276°-282° C.; CIMS (1% ammonia in methane): m/z (relative intensity) 279 (MH+, 54), 280 (MH+ +1, 100).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05733913 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-eedfd839ca854dbab9b143c699ca72ca |
| 출처 메모 | uspto-grants-1998_03 |