HCID 22314151, 화합물 → Allyl-{1,1-dimethyl-3-[3-(4-trifluoromethyl-phenyl)-benzo[d]isothiazol-6-yl]-prop-2-ynyl}-methyl-amine
반응식
[F:1][C:2]([F:27])([F:26])[C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:13]3[CH:14]=[CH:15][C:16](OS(C(F)(F)F)(=O)=O)=[CH:17][C:12]=3[S:11][N:10]=2)=[CH:5][CH:4]=1.[CH2:28]([N:31]([C:33]([CH3:37])([CH3:36])[C:34]#[CH:35])[CH3:32])[CH:29]=[CH2:30]>>[CH2:28]([N:31]([C:33]([CH3:37])([CH3:36])[C:34]#[C:35][C:16]1[CH:15]=[CH:14][C:13]2[C:9]([C:6]3[CH:7]=[CH:8][C:3]([C:2]([F:27])([F:26])[F:1])=[CH:4][CH:5]=3)=[N:10][S:11][C:12]=2[CH:17]=1)[CH3:32])[CH:29]=[CH2:30]참가 물질
3
실험 절차
In analogy to example 14.1, Trifluoro-methanesulfonic acid 3-(4-trifluoromethyl-phenyl)-benzo[d]isothiazol-6-yl ester and Allyl-(1,1-dimethyl-prop-2-ynyl)-methyl-amine were converted to yield Allyl-{1,1-dimethyl-3-[3-(4-trifluoromethyl-phenyl)-benzo[d]isothiazol-6-yl]-prop-2-ynyl}-methyl-amine as brown oil, MS: 415 (MH+).
출처 및 근거
- ORD 기록
- ord-7520442a6cc24df7842783990dbddcf2