Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuric Acid → HCID 178512812, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2-Methyl-2-thiopseudourea | HCID 5142 | — |
| 반응물 | Hexamethylenediamine | HCID 16402 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178512812 | HCID 178512812 | — |
반응 단계
To 2.3 g. of 1,6-diaminohexane dissolved in 50 ml. of H2O was added dropwise with vigorous stirring a solution of 2 g. of S-methylthiopseudourea.H2SO4 in 20 ml. of H2O. After the completion of addition, the stirring was continued for 15 hours, after which the precipitate (the diadduct) was filtered. The filtrate was concentrated to a viscous oil which upon the addition of 50 ml. of MeOH precipitated 718 mg. of white powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04762949 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-9cf58c54b4b744f8a9806c38daf1df95 |
| 출처 메모 | uspto-grants-1988_08 |