Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- → 2,4-Diamino-6-(5-aminopentyl)-1,3,5-triazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- | HCID 75657 | — |
| 반응물 | Carbamimidamidomethanimidamide | HCID 176517607 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2,4-Diamino-6-(5-aminopentyl)-1,3,5-triazine | HCID 21298790 | — |
반응 단계
A mixture of biguanide (1.05 g.), 4,5,6,7-tetrahydro-2-methoxy-3H-azepine (1.27 g.) and ethanol (50 ml.) was heated under reflux for 18 hours, cooled and the solid that crystallised was collected to give 2,4-diamino-6-(5-aminopentyl)-1,3,5-triazine which was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04762932 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-d160538931fd480d9675ac1086279244 |
| 출처 메모 | uspto-grants-1988_08 |