참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Benzene, (triethoxymethyl)- | HCID 74268 | — |
| 반응물 | 5-Butyryl-2-indolinone | HCID 23559378 | — |
| 생성물 | 1-Acetyl-5-butyryl-3-(ethoxy-phenyl-methylidene)-2-indolinone | HCID 68993053 | — |
반응 단계
10 g (49 mmol) 5-butyryl-2-indolinone (Ex. I.2) in 200 ml acetic anhydride are stirred for 5 h at 130° C. Then 35 ml triethyl orthobenzoate are added and the mixture is stirred for a further 4 h at 100° C. It is then evaporated down and the resulting precipitate is suction filtered, washed and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07176231B2 |
|---|
| 출처 데이터셋 | uspto-grants-2007_02 |
|---|
| ORD ID | ord-8abcb86c2e68461dac488cb4954908da |
|---|
| 출처 메모 | uspto-grants-2007_02 |
|---|
