Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → 1-Acetyl-5-isobutyryl-3-(ethoxy-phenyl-methylidene)-2-indolinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Benzene, (triethoxymethyl)- | HCID 74268 | — |
| 반응물 | 5-Isobutyryloxindole | HCID 21084646 | — |
| 용매 | Cyclohexane ethyl acetate methanol | HCID 22064753 | — |
| 생성물 | 1-Acetyl-5-isobutyryl-3-(ethoxy-phenyl-methylidene)-2-indolinone | HCID 68995758 | — |
반응 단계
Prepared from 5-isobutyryl-2-indolinone, acetic anhydride and triethyl orthobenzoate Rf=0.55 (silica gel, ethyl acetate/cyclohexane/methanol 9:9:2)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07176231B2 |
| 출처 데이터셋 | uspto-grants-2007_02 |
| ORD ID | ord-316ac5a9490846f384ba25ac601e1cdc |
| 출처 메모 | uspto-grants-2007_02 |