Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosphorus oxychloride → HCID 14256186, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosphorus oxychloride | HCID 24813 | — |
| 반응물 | 1-Bromo-2-propanol | HCID 29740 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | HCID 14256186 | HCID 14256186 | 42.2% |
반응 단계
To a solution of 46 g of phosphorus oxychloride in 110 ml of carbon tetrachloride was added with stirring 21 g of 1-bromo-2-propanol. The mixture was stirred overnight, the solvent removed and the residue evaporated twice from toluene at 35° C., then evaporated to dryness giving a dark oil. This oil was distilled on a Kugelrohr at 75° C., 0.3 mm giving 16.3 g of the desired compound as a white oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04762942 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-e3ab952f95f3447d8425a816cc6768d0 |
| 출처 메모 | uspto-grants-1988_08 |