2-(4-Benzyloxybenzyl)-2-phenoxybutyric acid ethyl ester → HCID 69320315, 화합물

HRID 348346노트

반응식

HRID 348346 반응식
[CH2:1]([O:3][C:4](=[O:30])[C:5]([CH2:15][C:16]1[CH:21]=[CH:20][C:19]([O:22]CC2C=CC=CC=2)=[CH:18][CH:17]=1)([O:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[CH2:6][CH3:7])[CH3:2]>C(OCC)(=O)C.[Pd]>[CH2:1]([O:3][C:4](=[O:30])[C:5]([CH2:15][C:16]1[CH:17]=[CH:18][C:19]([OH:22])=[CH:20][CH:21]=1)([O:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[CH2:6][CH3:7])[CH3:2]

참가 물질

4

반응물 1

HCID 693525592-(4-Benzyloxybenzyl)-2-phenoxybutyric acid ethyl ester

생성물 1

HCID 69320315HCID 69320315, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 8857Ethyl Acetate용매

실험 절차

2-(4-Benzyloxybenzyl)-2-phenoxybutyric acid ethyl ester (2.1 mmol) was dissolved in ethyl acetate (30 mL) and treated with 5% palladium on carbon (300 mg), and stirred under an atmosphere of hydrogen for 20 h. The suspension was filtered through celite and concentrated in vacuo to an oil.

후처리

  1. filtrationThe suspension was filtered through celite and
  2. concentrationconcentrated in vacuo to an oil

출처 및 근거

ORD 기록
ord-d89504f04e2c4c2a9509b7f36739a44e
출처 데이터셋
uspto-grants-2007_02
특허 번호
US07176224B2

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