Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trimethyl orthoformate → Methyl 1-methyl-1H-benzo[d]imidazole-5-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trimethyl orthoformate | HCID 9005 | — |
| 반응물 | Methyl 3-amino-4-(methylamino)benzoate | HCID 15586064 | — |
| 생성물 | Methyl 1-methyl-1H-benzo[d]imidazole-5-carboxylate | HCID 965319 | — |
반응 단계
A solution of methyl 3-amino-4-methylaminobenzoate (prepared as in DE 1990390463 A1) (2.57 g, 14 mmol) in trimethyl orthoformate (50 mL) was refluxed for 16 hours. The solvent was then removed under reduced pressure to afford 2.31 g of product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07176322B2 |
| 출처 데이터셋 | uspto-grants-2007_02 |
| ORD ID | ord-32dc8e7f00a3425182a33ced2a8f8734 |
| 출처 메모 | uspto-grants-2007_02 |