Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(Hydroxymethyl)isoquinoline → Isoquinoline-1-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(Hydroxymethyl)isoquinoline | HCID 2776247 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | Isoquinoline-1-carbaldehyde | HCID 265306 | 85.1% |
반응 단계
Isoquinolin-1-yl-methanol (123.7 mg) was dissolved in chloroform (6.2 ml) and then added with manganese dioxide (chemically processed product) (1.24 g), followed by stirring at room temperature for 30 minutes. The reaction solution was filtrated through Celite and the solvent was then distilled off. The residue was dried under vacuum, thereby obtaining the subject compound (103.9 mg) as a brown solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07176227B2 |
| 출처 데이터셋 | uspto-grants-2007_02 |
| ORD ID | ord-08bcf8622f984d33a60644c8f0c66571 |
| 출처 메모 | uspto-grants-2007_02 |