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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 348883생성일: 2026년 10월 26일

Methanol → 3-[5-(3-Methoxy-3-oxopropyl)-1,3-oxazol-2-yl]benzoic acid

https://huagongshe.com/reaction/348883

반응식

참여 물질

역할이름HCID투입량
반응물MethanolHCID 887—
반응물Thionyl ChlorideHCID 24386—
반응물3-[5-(2-Carboxyethyl)-1,3-oxazol-2-yl]benzoic acidHCID 21085690—
생성물3-[5-(3-Methoxy-3-oxopropyl)-1,3-oxazol-2-yl]benzoic acidHCID 21085691—

반응 단계

To 3-[5-(2-carboxyethyl)-1,3-oxazol-2-yl]benzoic acid (317 mg, 1.2 mmol) in methanol (5 mL) is added thionyl chloride (4.4 μL, 0.06 mmol), and the reaction is stirred at room temperature 16 h. The solution is concentrated under reduced pressure to give the title compound. ESI MS m/z 274.1 [M−H]−.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07176242B2
출처 데이터셋uspto-grants-2007_02
ORD IDord-c873f96b4449495daa857fc40856a66d
출처 메모uspto-grants-2007_02