Triethylamine → HCID 22139808, 화합물
반응식
[C:1]([NH:4][C:5]1[C:9]([Cl:10])=[C:8](Cl)[S:7][C:6]=1[C:12]([O:14][CH3:15])=[O:13])(=[O:3])[CH3:2].C(N(CC)CC)C>CO.[Pd]>[C:1]([NH:4][C:5]1[C:9]([Cl:10])=[CH:8][S:7][C:6]=1[C:12]([O:14][CH3:15])=[O:13])(=[O:3])[CH3:2]참가 물질
5
실험 절차
was obtained by catalytically hydrogenating a mixture of 25 g of methyl 3-acetylamino-4,5-dichlorothiophene-2-carboxylate in 300 ml of methanol, 9.5 g of triethylamine and with 10 g of palladium on carbon and room temperature and 760 mmHg column (standard pressure conditions). After the calculated amount of hydrogen had been absorbed, the catalyst was filtered off, the solvent was distilled off on a Rotavapor and the product was crystallized under water.
후처리
- customwas obtained by catalytically hydrogenating
- customAfter the calculated amount of hydrogen had been absorbed
- filtrationthe catalyst was filtered off
- distillationthe solvent was distilled off on a Rotavapor
- customthe product was crystallized under water
출처 및 근거
- ORD 기록
- ord-3d1a83c62a774dabbb0f41561cafa9b7
- 출처 데이터셋
- uspto-grants-2007_02
- 특허 번호
- US07179830B2
반응 노트
불러오는 중…