Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 5-Bromofuran-2-carbonyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 5-Bromo-2-furanecarboxylic acid | HCID 68511 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 5-Bromofuran-2-carbonyl chloride | HCID 2757011 | — |
반응 단계
21.0 g of 5-bromo-2-furancarboxylic acid were suspended in 650 ml of toluene and 40 ml of thionyl chloride and the suspension was heated to reflux for 2 hours. The reaction solution was thereafter concentrated, whereby 5-bromo-2-furancarboxylic acid chloride was obtained as the residue.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04764522 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-374bfbb4f33346df9af44276ccb38c16 |
| 출처 메모 | uspto-grants-1988_08 |