Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalic acid dihydrate → N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide oxalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalic acid dihydrate | HCID 61373 | — |
| 반응물 | N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide | HCID 67930011 | — |
| 생성물 | N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide oxalate | HCID 67930072 | 80% |
반응 단계
The procedure of Example 7 was repeated using 917 mg (2.36 mmol.) of N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide and 298 mg (2.36 mmol.) of oxalic acid dihydrate, to obtain 901 mg (yield: 80%) of the subject compound as a whilte crystalline product upon recrystallization from 8 ml of ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04764617 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-d189332df8ad49bc8a8152b0d3067aa0 |
| 출처 메모 | uspto-grants-1988_08 |