Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diphenylamine → Triphenylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diphenylamine | HCID 11487 | — |
| 반응물 | Iodobenzene | HCID 11575 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 촉매 | Copper | HCID 23978 | — |
| 생성물 | Triphenylamine | HCID 11775 | 82% |
반응 단계
The same equipment and conditions as in example I were employed with the following charge: 20.4 grams (0.1 mole) iodobenzene, 27.4 grams (0.15 mole) diphenylamine, 16.8 grams (0.3 mole) potassium hydroxide flakes, 15.0 grams of copper powder and 30.0 milliliters of Soltrol® 170. The above-identified product was obtained as colorless crystals having a melting point of 125°-126° C. Yield 82%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04764625 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-05bdd44fe3d447eaafc64f1cc325b326 |
| 출처 메모 | uspto-grants-1988_08 |