Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl N-cyanodithioiminocarbonate → methyl N-cyano-1-methyl-2-(phenylmethylene)-hydrazinecarboximidothioate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl N-cyanodithioiminocarbonate | HCID 66289 | — |
| 반응물 | Benzaldehyde Methylhydrazone | HCID 302615 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | methyl N-cyano-1-methyl-2-(phenylmethylene)-hydrazinecarboximidothioate | HCID 54323404 | — |
반응 단계
A mixture of cyanocarbonimidodithioic acid dimethyl ester (1.46 g) and benzaldehyde N-methyl hydrazone (1.34 g) in acetonitrile was heated under reflux for 50 hr. The reaction mixture was cooled to 25° to give the title compound as colourless crystals, m.p. 132°-133° (0.73 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04764612 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-5a4c884a205c4c5d87920b320e7a65e5 |
| 출처 메모 | uspto-grants-1988_08 |