Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylhydrazine → N-cyano-1-methylhydrazinecarboximidothioic acid methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylhydrazine | HCID 6061 | — |
| 반응물 | Dimethyl N-cyanodithioiminocarbonate | HCID 66289 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N-cyano-1-methylhydrazinecarboximidothioic acid methyl ester | HCID 86738283 | — |
반응 단계
A mixture of methyl hydrazine (0.48 ml) and cyanocarbonimidodithioic acid dimethyl ester (1.3 g) in acetonitrile was stirred at 25° for 16 hours. The resulting solution was evaporated to a gum which was crystallised from acetonitrile/ether to give the title compound as colourless granules (210 mg) m.p. 69°-71°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04764612 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-3d31bfcbc0f843ba9ecffef034de6c02 |
| 출처 메모 | uspto-grants-1988_08 |