Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl N-cyanodithioiminocarbonate → HCID 178503919, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl N-cyanodithioiminocarbonate | HCID 66289 | — |
| 반응물 | 3-{3-[(Pyrrolidin-1-yl)methyl]phenoxy}propan-1-amine | HCID 12797454 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | HCID 178503919 | HCID 178503919 | — |
반응 단계
A solution of N-cyano-carbonimidodithioic acid dimethyl ester (5 g) in ethyl acetate (50 ml) was added to a solution of 3-[3-(1-pyrrolidinylmethyl)phenoxy]propanamine in ethyl acetate (60 ml). The reaction mixture was stirred at room temperature for 1 hr to give the title compound as an off-white solid m.p. 107°-108.5° (7.45 g). TLC silica; ethyl acetate: isopropanol:water:0.88 ammonia (25:15:8:2) single spot Rf 0.7.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04764612 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-8e99aae1d1e04736be34c3bafe85fee5 |
| 출처 메모 | uspto-grants-1988_08 |