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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 350651생성일: 2026년 10월 26일

3-Benzyloxy-4-methoxypicolinic acid → 3-Hydroxy-4-methoxypyridine-2-carboxylic acid

https://huagongshe.com/reaction/350651

반응식

참여 물질

역할이름HCID투입량
반응물3-Benzyloxy-4-methoxypicolinic acidHCID 19960289—
촉매HCID 178418390HCID 178418390—
용매EthanolHCID 702—
생성물3-Hydroxy-4-methoxypyridine-2-carboxylic acidHCID 1104112181.6%

반응 단계

3-Benzyloxy-4-methoxypicolinic acid (5.3 g) was suspended in 25 ml of ethanol. 10% palladium-carbon (0.5 g) was added to the suspension. The mixture was then catalytically hydrogenated under atmospheric pressure for 30 min. The reaction solution was filtered under the reduced pressure. The filtrate was concentrated under the reduced pressure to give 2.8 g (yield 81.6%) of the title compound as colorless powder.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07183278B1
출처 데이터셋uspto-grants-2007_02
ORD IDord-fdccc608141d4e1c8f6a5004e9b1d6cb
출처 메모uspto-grants-2007_02