Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexane → 4-Aza-4-cyclohexyl-2-(4-nitrophenyl)-1,6-heptadiene-3,5-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | Acrylamide, N-cyclohexyl- | HCID 137811 | — |
| 반응물 | 2-(4-Nitrophenyl)prop-2-enoic acid | HCID 13278029 | — |
| 생성물 | 4-Aza-4-cyclohexyl-2-(4-nitrophenyl)-1,6-heptadiene-3,5-dione | HCID 20027806 | — |
반응 단계
The title compound is prepared analogously to Example 1c starting from 40.5 g of a-(4-nitrophenyl)-acrylic acid, 26.7 g of oxalyl chloride and 26.8 g of N-cyclohexylacrylamide. Melting point 73°-74° (from hexane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04764640 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-e662789599884e72a40dfc84bcd03121 |
| 출처 메모 | uspto-grants-1988_08 |