Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 4-((Allyl(methyl)amino)methyl)thiazol-2-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | N-Methylallylamine | HCID 69391 | — |
| 반응물 | 2-Thiazolamine, 4-(chloromethyl)-, hydrochloride (1:1) | HCID 73228 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-((Allyl(methyl)amino)methyl)thiazol-2-amine | HCID 21090603 | — |
반응 단계
N-allyl-N-methylamine (7.0 mg, 0.1 mmol), 2-amino-4-chloromethylthiazole hydrochloride (18.5 mg, 0.1 mmol), and potassium carbonate (30 mg, 0.21 mmol) are shaken in ethanol (1 mL) at room temperature for 18 hours. The mixture is filtered and the filtrate was condensed under vacuum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07183300B2 |
| 출처 데이터셋 | uspto-grants-2007_02 |
| ORD ID | ord-6de76e9d87074e8c81db3041feaa73dd |
| 출처 메모 | uspto-grants-2007_02 |