Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl perfluorobutyl ether → Butane, 1-(chloromethoxy)-1,1,2,2,3,3,4,4,4-nonafluoro-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl perfluorobutyl ether | HCID 164514 | — |
| 반응물 | Butane, 1-(chloromethoxy)-1,1,2,2,3,3,4,4,4-nonafluoro- | HCID 9925852 | — |
| 반응물 | HCID 131724435 | HCID 131724435 | — |
| 생성물 | Butane, 1-(chloromethoxy)-1,1,2,2,3,3,4,4,4-nonafluoro- | HCID 9925852 | — |
| 생성물 | C4F9OCHCl2 | HCID 9927029 | — |
반응 단계
GLC at the conclusion of the addition showed the following C4F9OCH3(5%), C4F9OCH2Cl (65%) and C4F9OCHCl2 HCl2 (29%) and C4F9OCCl3 (0.2%). The reaction solution was washed first with dilute aqueous potassium hydroxide, and then with water, and distilled using a 40-plate perforated plate column to yield C4F9OCH2Cl, b.p.=87° C. and C4F9OCHCl2, b.p.=96° C. in purifies of about 99%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06743262B1 |
| 출처 데이터셋 | uspto-grants-2004_06 |
| ORD ID | ord-75b885c6c38e4e7893cd358e501abbe0 |
| 출처 메모 | uspto-grants-2004_06 |