Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium ethanethiolate → ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium ethanethiolate | HCID 4459711 | — |
| 반응물 | 5,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile | HCID 19833886 | — |
| 용매 | Ethanethiol | HCID 6343 | — |
| 생성물 | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate | HCID 20041719 | — |
반응 단계
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and sodium ethanethiolate in ethanethiol there is obtained ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate and therefrom with hydrochloric acid in alcohol there is obtained the hydrochloride, m.p. 220° C. (with decomposition);
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04766115 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-9b579c6ea71c44829cf397c559a47b98 |
| 출처 메모 | uspto-grants-1988_08 |