Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2-Methylindol-4-yloxyacetic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 1,4-Dioxane | HCID 31275 | — |
| 반응물 | 2-Methylindol-4-yloxyacetic Acid Methyl Ester | HCID 69130376 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-Methylindol-4-yloxyacetic Acid | HCID 69589397 | 69.2% |
반응 단계
To a solution of 2-methylindol-4-yloxyacetic acid methyl ester (5.4 g) in methanol (18 ml)—dioxane (36 ml) was added 5N aqueous solution of sodium hydroxide (15 ml), and the mixture was stirred at room temperature for 1 hour. To the reaction solution was added 2N hydrochloric acid to give the title compound (3.5 g) having the following physical data.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06743793B2 |
| 출처 데이터셋 | uspto-grants-2004_06 |
| ORD ID | ord-e9bd21d5ed624234a0963aa400119c60 |
| 출처 메모 | uspto-grants-2004_06 |