Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → 3,4-Dihydro-2H-1,4-benzoxazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 2H-1,4-benzoxazin-3(4H)-one | HCID 72757 | — |
| 반응물 | Diboron | HCID 6328200 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 3,4-Dihydro-2H-1,4-benzoxazine | HCID 585096 | — |
반응 단계
3,4-Dihydro-3-oxo-1,4(2H)-benzoxazine was refluxed for several hours in one equivalent of diborane in tetrahydrofuran. Excess sodium hydroxide solution was added, the product was extracted with ether and the solvent was evaporated to give the title compound as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04766118 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-4e559cf6b812488bb588a627a636cd16 |
| 출처 메모 | uspto-grants-1988_08 |