4-Fluoro-3-methoxybenzaldehyde → HCID 22714661, 화합물

반응식

[CH3:1][S:2]([C:4]1[CH:10]=[CH:9][C:7]([NH2:8])=[CH:6][CH:5]=1)=[O:3].[F:11][C:12]1[CH:19]=[CH:18][C:15]([CH:16]=O)=[CH:14][C:13]=1[O:20][CH3:21]>>[F:11][C:12]1[CH:19]=[CH:18][C:15]([CH:16]=[N:8][C:7]2[CH:9]=[CH:10][C:4]([S:2]([CH3:1])=[O:3])=[CH:5][CH:6]=2)=[CH:14][C:13]=1[O:20][CH3:21]

참가 물질

반응물 2

HCID 27373584-Fluoro-3-methoxybenzaldehyde

HCID 114350654-Methanesulfinylaniline

생성물 1

HCID 22714661HCID 22714661, 화합물

실험 절차

Following a similar procedure to that described in section a of example 1, but starting from 4-methylsulfinylaniline (obtained in reference example 2) instead of 4-methylsulfonylaniline and from 4-fluoro-3-methoxybenzaldehyde instead of 4-isopropoxybenzaldehyde, the desired compound was obtained, which was directly used in the next step.

출처 및 근거

ORD 기록: ord-44ce878267544bcaaefb565f16cccd39
출처 데이터셋: uspto-grants-2004_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06743816B2

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