참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | 2-Bromonaphthalene | HCID 11372 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 용매 | Nitrobenzene | HCID 7416 | — |
| 생성물 | 1-(6-Bromonaphthalen-2-yl)ethanone | HCID 12433082 | — |
반응 단계
A mixture of 41.4 g of 2-bromonaphthalene, 15.7 g of acetyl chloride and 28 g of aluminum chloride in 250 ml of nitrobenzene was stirred at 100° C. for 4 hours. The reaction mixture was poured onto ice water and the resulting solid filtered off, washed with water and distilled under reduced pressure. The distillate was recrystallized from hexane to yield 2-bromo-6-acetylnaphthalene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04766127 |
|---|
| 출처 데이터셋 | uspto-grants-1988_08 |
|---|
| ORD ID | ord-6b8ce0e0912b4f5087e0b932e9425f44 |
|---|
| 출처 메모 | uspto-grants-1988_08 |
|---|
