2-Allylphenol → Benzoxazines

HRID 351950

반응식

HRID 351950 반응식
[NH2:1][CH2:2][CH2:3][CH2:4][Si](OC)(OC)OC.[CH2:12]([C:15]1C=CC=C[C:16]=1[OH:21])[CH:13]=[CH2:14]>C1(C)C=CC=CC=1>[O:21]1[C:16]2[CH:15]=[CH:12][CH:13]=[CH:14][C:4]=2[CH:3]=[CH:2][NH:1]1

참가 물질

4

반응물 2

HCID 156242-AllylphenolHCID 83756Aminopropyltrimethoxysilane

생성물 1

HCID 17845026Benzoxazines수율 94%

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

This compound was prepared according to the method described in the previous examples using 3-aminopropyltrimethoxysilane (17.9 g, 100 mmole), paraformaldehade (6.3 g, 210 mmole), 2-allyl-phenol (13.4 g, 0.1 mmole), and toluene (200 ml). The final product was obtained as a slightly yellow, mobile liquid. The yield was 94% of theory.

후처리

  1. customThis compound was prepared

출처 및 근거

ORD 기록
ord-6358ad625d7f4fa781932705f29eec87
출처 데이터셋
uspto-grants-2004_06
특허 번호
US06743852B2

연결된 노트

불러오는 중…