4-Pyridin-3-yl-benzoic acid → 4-tert-Butoxycarbonyl-2-ethoxycarbonyl-1-[4-(3-pyridyl)benzoyl]piperazine

HRID 352740

반응식

HRID 352740 반응식
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7]2[CH:15]=[CH:14][C:10]([C:11]([OH:13])=O)=[CH:9][CH:8]=2)[CH:2]=1.[C:16]([O:20][C:21]([N:23]1[CH2:28][CH2:27][NH:26][CH:25]([C:29]([O:31][CH2:32][CH3:33])=[O:30])[CH2:24]1)=[O:22])([CH3:19])([CH3:18])[CH3:17]>>[C:16]([O:20][C:21]([N:23]1[CH2:28][CH2:27][N:26]([C:11](=[O:13])[C:10]2[CH:9]=[CH:8][C:7]([C:3]3[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=3)=[CH:15][CH:14]=2)[CH:25]([C:29]([O:31][CH2:32][CH3:33])=[O:30])[CH2:24]1)=[O:22])([CH3:19])([CH3:18])[CH3:17]

참가 물질

3

반응물 2

HCID 15152444-Pyridin-3-yl-benzoic acidHCID 114026711-tert-Butyl 3-ethyl piperazine-1,3-dicarboxylate

생성물 1

HCID 177964714-tert-Butoxycarbonyl-2-ethoxycarbonyl-1-[4-(3-pyridyl)benzoyl]piperazine

실험 절차

In the same manner as in Referential Example 12, a reaction was conducted using 4-(3-pyridyl)benzoic acid and 1-tert-butoxycarbonyl-3-ethoxycarbonylpiperazine as starting materials, whereby the title compound was obtained.

출처 및 근거

ORD 기록
ord-e8ae6db69c474385ac7dd1e619ff5203
출처 데이터셋
uspto-grants-2004_06
특허 번호
US06747023B1

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