Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → HCID 22708122, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 3-Fluoroacetophenone | HCID 9967 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 3-Fluorobenzaldehyde | HCID 68009 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 22708122 | HCID 22708122 | 93% |
반응 단계
A mixture of 3-fluorobenzaldehyde (7.63 mL, 72.4 mmol), 3-fluoroacetophenone (10 g, 72.4 mmol), potassium hydroxide (5.18 g, 92.6 mmol), ethanol (23 mL) and water (47 mL) was stirred overnight at room temperature. After the reaction solution was diluted with water, the solid was collected by filtration and washed with ethanol and diethyl ether, to give the title compound (16.4 g, 93%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06750232B2 |
| 출처 데이터셋 | uspto-grants-2004_06 |
| ORD ID | ord-1dc89752ecc94f6f816c4c7f12c5b1be |
| 출처 메모 | uspto-grants-2004_06 |