Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Chloro-2-pentyne → (4-Pent-2-ynyloxy-phenylsulfanyl)-acetic acid ethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Chloro-2-pentyne | HCID 89764 | — |
| 반응물 | Ethyl 2-[(4-hydroxyphenyl)sulfanyl]acetate | HCID 3742252 | — |
| 생성물 | (4-Pent-2-ynyloxy-phenylsulfanyl)-acetic acid ethyl ester | HCID 11288950 | — |
반응 단계
(4-Pent-2-ynyloxy-phenylsulfanyl)-acetic acid ethyl ester was prepared according to the general method as outlined in Example 1 (Step 2). Starting from (4-hydroxy-phenylsulfanyl)-acetic acid ethyl ester (5 g, 30 mmol) and 2-pentynyl chloride (3.7 g, 36.6 mmol) 7.15 g of the product isolated. Yield 7.15 g (86%); brown oil; MS: 278 EI (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06753337B2 |
| 출처 데이터셋 | uspto-grants-2004_06 |
| ORD ID | ord-457da6cdbe504dcfa39327d4fe30e426 |
| 출처 메모 | uspto-grants-2004_06 |