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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 353695생성일: 2026년 10월 25일

Thioglycolic Acid → Ethyl 4-carboxymethylsulfenyl-2-chlorobenzoate

https://huagongshe.com/reaction/353695

반응식

참여 물질

역할이름HCID투입량
반응물Thioglycolic AcidHCID 1133—
반응물Potassium CarbonateHCID 11430—
반응물Benzoic acid, 2,4-dichloro-, ethyl esterHCID 42026—
용매DimethylformamideHCID 6228—
생성물Ethyl 4-carboxymethylsulfenyl-2-chlorobenzoateHCID 12993801—

반응 조건

온도80 °C

반응 단계

A mixture containing ethyl 2,4-dichlorobenzoate (10.0 g), potassium carbonate (9.44 g), dimethylformamide (50 ml), and mercaptoacetic acid (3.8 ml) was allowed to react with heat at 80° C. for 4 hours.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06756343B1
출처 데이터셋uspto-grants-2004_06
ORD IDord-c042bd80104540ff8b5020c5211258d2
출처 메모uspto-grants-2004_06