Thioglycolic Acid → Ethyl 4-carboxymethylsulfenyl-2-chlorobenzoate
반응식
[Cl:1][C:2]1[CH:12]=[C:11](Cl)[CH:10]=[CH:9][C:3]=1[C:4]([O:6][CH2:7][CH3:8])=[O:5].C(=O)([O-])[O-].[K+].[K+].[SH:20][CH2:21][C:22]([OH:24])=[O:23]>CN(C)C=O>[C:22]([CH2:21][S:20][C:11]1[CH:10]=[CH:9][C:3]([C:4]([O:6][CH2:7][CH3:8])=[O:5])=[C:2]([Cl:1])[CH:12]=1)([OH:24])=[O:23]참가 물질
5
반응 조건
- 온도
- 80 °C
실험 절차
A mixture containing ethyl 2,4-dichlorobenzoate (10.0 g), potassium carbonate (9.44 g), dimethylformamide (50 ml), and mercaptoacetic acid (3.8 ml) was allowed to react with heat at 80° C. for 4 hours.
후처리
- customto react
출처 및 근거
- ORD 기록
- ord-80dc97ce6d084062a119638e87f00d1a
- 출처 데이터셋
- uspto-grants-2004_06
- 특허 번호
- US06756343B1
반응 노트
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