반응식
FOC(F)(F)F.FOC(OF)(F)F.F[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[NH:21][S:22]([CH3:25])(=[O:24])=[O:23].FC1C=CC(NS(C)(=O)=O)=CC=1.FC1C=C(F)C=CC=1NS(C)(=O)=O.FC1C=CC=C(F)C=1NS(C)(=O)=O>>[C:16]1([NH:21][S:22]([CH3:25])(=[O:24])=[O:23])[CH:15]=[CH:20][CH:19]=[CH:18][CH:17]=1참가 물질
7
반응물 6
생성물 1
실험 절차
The procedure of Example 26 was repeated except that in place of the fluoroxytrifluoromethane, there was added bis-(fluoroxy)difluoromethane at a rate of 2.40 parts per hour for one hour. Analysis of the reaction product by liquid chromatographic techniques indicated 38% N-(2-fluorophenyl)methanesulfonamide, 12% N-(4-fluorophenyl)methanesulfonamide, 10% N-(2,4-difluorophenyl)methanesulfonamide and 1% N-(2,6-difluorophenyl)methanesulfonamide at 97% conversion.
출처 및 근거
- ORD 기록
- ord-760c8144346a4e968d0ba51e241675e6
- 출처 데이터셋
- uspto-grants-1988_08
- 특허 번호
- US04766243
연결된 노트
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