Cyanuric chloride → 3-Chlorooctane

반응식

[CH3:1][CH2:2][CH:3](O)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].N1C(Cl)=NC(Cl)=NC=1[Cl:12]>>[Cl:12][CH:3]([CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH2:2][CH3:1]

참가 물질

반응물 2

HCID 7954Cyanuric chloride

HCID 115273-Octanol

생성물 1

HCID 335753-Chlorooctane

실험 절차

Using a procedure analogous to that of Example 1, 81 g (0.522 mol) of 3-octanol is reacted with 62.1 g (0.337 mol) of cyanuric chloride over a period of 9 hours at a reaction temperature of 70° C. The liquid reaction phase after extraction with sodium hydroxide has the following composition:

후처리

customThe liquid reaction phase
extractionafter extraction with sodium hydroxide

출처 및 근거

ORD 기록: ord-a64555b8c0f043069480e86d2d585f4e
출처 데이터셋: uspto-grants-2004_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06756513B2

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