Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Anthranilic Acid → 2-Amino-4-methoxybenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Anthranilic Acid | HCID 227 | — |
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | 4-Methoxy-2-nitrobenzoic acid | HCID 288657 | — |
| 생성물 | 2-Amino-4-methoxybenzoic acid | HCID 351010 | — |
반응 단계
A solution of 4-methoxy-2-nitrobenzoic acid (19.3 g., 97.9 mmole) of 200 ml. 1 N NH4OH was reduced overnight in presence of 5% Pd/BaCO3. The reaction mixture was filtered and acidified with acetic acid to yield 15.8 g. (96%) of the anthranilic acid, M.P. 186°-188° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04377581 |
| 출처 데이터셋 | uspto-grants-1983_03 |
| ORD ID | ord-50a7b5b4e30d473090bcc1d5854a60ba |
| 출처 메모 | uspto-grants-1983_03 |