Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium hydride → HCID 12961164, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 5-Nitro-2,3-dihydro-1,3-benzoxazol-2-one | HCID 263965 | — |
| 반응물 | Methyl 8-bromooctanoate | HCID 11107373 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 12961164 | HCID 12961164 | — |
반응 단계
The product is produced as described in example 1 from 6 g. of NaH (80% suspension in mineral oil), 36 g. of 5-nitrobenzoxazolin-2-one (produced in usual manner by reacting 2-amino-4-nitrophenol-hydrochloride with phosgene), 400 cc. of DMF, 47.4 g. of 8-bromo caprylic acid methyl ester and 6 g. of NaJ.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04377695 |
| 출처 데이터셋 | uspto-grants-1983_03 |
| ORD ID | ord-5083d77515734e688cceec493cc3548a |
| 출처 메모 | uspto-grants-1983_03 |