Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Pyridinemethanol → [(2-Methylphenyl)diphenylphosphoranylidene]carbamic acid, 3-pyridinylmethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Pyridinemethanol | HCID 7510 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 1-[[[(2-methylphenyl)diphenylphosphoranylidene]amino]carbonyl]-1H-imidazole | HCID 14771280 | — |
| 용매 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 생성물 | [(2-Methylphenyl)diphenylphosphoranylidene]carbamic acid, 3-pyridinylmethyl ester | HCID 14280261 | — |
반응 단계
A 760 mg portion of 3-pyridinemethanol, 35 ml of 1,2-dimethoxyethane, 340 mg of 50% sodium hydride in oil and 2.7 g of 1-[[[(2-methylphenyl)diphenylphosphoranylidene]amino]carbonyl]-1H-imidazole were reacted as described in Example 8, giving 2.05 g of the desired product, mp 142°-143° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04767749 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-a2325ed719454bdf93b371ccb8466179 |
| 출처 메모 | uspto-grants-1988_08 |