Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methyl-3-buten-2-ol → 2,5-Dimethyl-2,5-hexanediol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methyl-3-buten-2-ol | HCID 8257 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | 2,5-Dimethyl-2,5-hexanediol | HCID 8031 | — |
반응 단계
2-Methyl-3-buten-2-ol, 2-propanol and tert.-butyl peroxy pivalate (75% solution in aliphates) are reacted in a molar ratio of 1:15:0.3 at 90° C. and a pressure of 500 kPa as described in example 1. After a contact period of 20 minutes of the reaction mixture in a tube reactor 95% of the olefin used has been converted. 2,5-dimethylhexane-2,5-diol is formed with a selectivity of 76%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05831134 |
| 출처 데이터셋 | uspto-grants-1998_11 |
| ORD ID | ord-eed7f6c0c9704090aaf4de213e18c8fa |
| 출처 메모 | uspto-grants-1998_11 |