2,8-Diacetylamino-1-tetralone → 2-Acetylamino-8-amino-5-methyl-1-tetralone

HRID 355963노트

반응식

HRID 355963 반응식
[C:1]([NH:4][CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([NH:16]C(=O)C)[CH:9]=[CH:10][C:11]=2[CH3:15])[C:6]1=[O:20])(=[O:3])[CH3:2].C(NC1CCC2C(=C(NC(=O)C)C=CC=2)C1=O)(=O)C>>[C:1]([NH:4][CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([NH2:16])[CH:9]=[CH:10][C:11]=2[CH3:15])[C:6]1=[O:20])(=[O:3])[CH3:2]

참가 물질

3

반응물 2

HCID 120472982,8-Diacetylamino-1-tetraloneHCID 867509612,8-Diacetylamino-5-methyl-1-tetralone

생성물 1

HCID 224494492-Acetylamino-8-amino-5-methyl-1-tetralone

실험 절차

The reaction was carried out in the same manner as in Example 1-(4), except that 400 mg of the compound prepared in (7) above was used instead of 2,8-diacetylamino-1-tetralone of Example 1-(4), and post-treated to produce 265 mg of the title compound.

후처리

  1. additionpost-treated

출처 및 근거

ORD 기록
ord-5c36ab79f2e04e778313519007891dd5
출처 데이터셋
uspto-grants-1998_11
특허 번호
US05834476

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