Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Acetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one → 1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Acetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one | HCID 10353298 | — |
| 반응물 | N-(8-Oxo-5,6,7,8-tetrahydronaphthalen-1-YL)acetamide | HCID 12119265 | — |
| 생성물 | 1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one | HCID 22449453 | — |
반응 단계
The reaction was carried out in the same manner as in Example 1-(2), except that 270 mg of the compound prepared in (2) above was used instead of 8-acetylamino-1-tetralone of Example 1-(2). The reaction mixture obtained by the post-treatment was further reacted in the same manner as in Example 1-(3) and post-treated to produce 126 mg of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05834476 |
| 출처 데이터셋 | uspto-grants-1998_11 |
| ORD ID | ord-a6c9eea160d542618b7334d21eca165d |
| 출처 메모 | uspto-grants-1998_11 |